CHEM 2212L Amide Synthesis Lab Report Worksheet Graded
Student
Kendall Kessler
Total Points
pts
Question 1
Amide Synthesis Lab pts
+ 6 pts Acetic Anhydride
Aluminum oxide
Ethyl acetate
+ 0 pts Incorrect
Question 2
Boiling Points pts
+ 4 pts Ethyl acetate 77oC
Acetic Anhydride 139-140oC
+ 0 pts Incorrect
Question 3
Melting Point pts
+ 2 pts Aluminum Oxide 2040-2072oC
+ 0 pts Incorrect
Question 4
Techniques pts
+ 10 pts Solid-Liquid Extraction or Liquid/Liquid Extraction (either is accepted)
Gravity Filtration
Recrystallization
IR Spectroscopy
1H NMR Spectroscopy
− 2 pts 1 missing/Incorrect
Question 5
Safety Pictograms pts
+ 8 pts Flammable
Corrosive
Acute Toxicity
Minor/Other Health Hazard
− 2 pts 1 missing/Incorrect
,Question 6
Glassware pts
+ 6 pts Graduated Cylinder (1pt)
Beaker (2pts)
Erlenmeyer Flask (2pts)
Glass Funnel (1pt)
− 1 pt 1 missing/Incorrect
,Question 7
Lab Procedure Questions pts
7.1 Final Product Structure pts
+ 3 pts
+ 0 pts Incorrect
7.2 Amide Synthesis Electrophile pts
+ 4 pts
+ 0 pts Incorrect
7.3 Amide Synthesis Nucleophile pts
+ 3 pts Primary Amine
+ 0 pts Incorrect
7.4 Amide Synthesis Catalyst pts
+ 4 pts Aluminum Oxide [Al2O3]
+ 0 pts Incorrect
7.5 Amide Synthesis Solvent pts
+ 4 pts
+ 0 pts Incorrect
, Question 8
Amide Synthesis Data Sheet pts
8.1 Unknown Amine Code pt
+ 1 pt Answer based on student’s lab data
+ 0 pts Incorrect
8.2 Volume of Unknown Amine pt
+ 1 pt Answer based on student’s lab data
+ 0 pts Incorrect
8.3 Volume of Glacial Acetic Acid pt
+ 1 pt 1.0mL (exact answer based on student data)
+ 0 pts Incorrect
8.4 Mass of Aluminum Oxide pt
+ 1 pt 0.153g (exact answer based on student data)
+ 0 pts Incorrect
8.5 Volume of Ethyl Acetate Extraction Solvent pt
+ 1 pt ~10mL (exact answer based on student data)
+ 0 pts Incorrect
8.6 Volume of Ethyl Acetate Wash pt
+ 1 pt ~5mL (exact answer based on student data)
+ 0 pts Incorrect
8.7 Weight of the Final Product pt
+ 1 pt Answer based on student’s lab data
+ 0 pts Incorrect
Student
Kendall Kessler
Total Points
pts
Question 1
Amide Synthesis Lab pts
+ 6 pts Acetic Anhydride
Aluminum oxide
Ethyl acetate
+ 0 pts Incorrect
Question 2
Boiling Points pts
+ 4 pts Ethyl acetate 77oC
Acetic Anhydride 139-140oC
+ 0 pts Incorrect
Question 3
Melting Point pts
+ 2 pts Aluminum Oxide 2040-2072oC
+ 0 pts Incorrect
Question 4
Techniques pts
+ 10 pts Solid-Liquid Extraction or Liquid/Liquid Extraction (either is accepted)
Gravity Filtration
Recrystallization
IR Spectroscopy
1H NMR Spectroscopy
− 2 pts 1 missing/Incorrect
Question 5
Safety Pictograms pts
+ 8 pts Flammable
Corrosive
Acute Toxicity
Minor/Other Health Hazard
− 2 pts 1 missing/Incorrect
,Question 6
Glassware pts
+ 6 pts Graduated Cylinder (1pt)
Beaker (2pts)
Erlenmeyer Flask (2pts)
Glass Funnel (1pt)
− 1 pt 1 missing/Incorrect
,Question 7
Lab Procedure Questions pts
7.1 Final Product Structure pts
+ 3 pts
+ 0 pts Incorrect
7.2 Amide Synthesis Electrophile pts
+ 4 pts
+ 0 pts Incorrect
7.3 Amide Synthesis Nucleophile pts
+ 3 pts Primary Amine
+ 0 pts Incorrect
7.4 Amide Synthesis Catalyst pts
+ 4 pts Aluminum Oxide [Al2O3]
+ 0 pts Incorrect
7.5 Amide Synthesis Solvent pts
+ 4 pts
+ 0 pts Incorrect
, Question 8
Amide Synthesis Data Sheet pts
8.1 Unknown Amine Code pt
+ 1 pt Answer based on student’s lab data
+ 0 pts Incorrect
8.2 Volume of Unknown Amine pt
+ 1 pt Answer based on student’s lab data
+ 0 pts Incorrect
8.3 Volume of Glacial Acetic Acid pt
+ 1 pt 1.0mL (exact answer based on student data)
+ 0 pts Incorrect
8.4 Mass of Aluminum Oxide pt
+ 1 pt 0.153g (exact answer based on student data)
+ 0 pts Incorrect
8.5 Volume of Ethyl Acetate Extraction Solvent pt
+ 1 pt ~10mL (exact answer based on student data)
+ 0 pts Incorrect
8.6 Volume of Ethyl Acetate Wash pt
+ 1 pt ~5mL (exact answer based on student data)
+ 0 pts Incorrect
8.7 Weight of the Final Product pt
+ 1 pt Answer based on student’s lab data
+ 0 pts Incorrect
