Solutions Manual For Descriptive Inorganic Chemistry 6th Edition By Rayner-Canham, Geoff 9781464125577

LaboratoryeManualeofePracticaleInorganiceIIeChemistry




Laboratorymanual Of e e




PRACTICALINORGANICII C
e e e




HEMISTRY


HCP




CCP



By:
M. Pranjoto Utomo
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DEPARTMENTeOFeCHEMISTRYeEDUCATIONeFACUL
TYeOFeMATHEMATICSeANDeNATURALeSCIENCES
YOGYAKARTAeSTATEeUNIVERSITYe201
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, LaboratoryeManualeofePracticaleInorganiceIIeChemistry


PREFACE



TheemanualeofeInorganiceIIelaboratoryeworkeiseaelaboratoryeguidelineetoetheestudentseofeC
hemistryeDepartment,eMathematicseandeNaturaleScienceseFaculty,eYogyakartaeStateeUniversi
ty,eineInorganiceIIecourse.eAccordingetoetheematerialeofeInorganiceIIecourse,etheelaboratoryeacti
vitieseareedirectedetoeunderstandetheemodeleofeionicecompoundecloseepacking,ereduction-
oxidationereactioneofeseveralemetals,eimproveetheedoubleesaltepreparationeandere-
crystallizationeskillseasetheebasiceforeadvanceelaboratoryeactivities.
e



Becauseeofetheerestrictivenesseofeequipmenteandechemicals,esomeeofepracticalesubjectecane
notebeedone.eOfecourse,ethiselaboratoryemanualedoesenotesupporteoptimallyetoetheeInorganiceIIec
ourse.
TheeEnglisheeditioneofeInorganiceIIelaboratoryeworkemanualeisetheesameeinecontentsewitheIn
donesianeedition.eRevisionedoneebyesimplifiesetheelanguageeandetheedirectionealsoeseparateseth
eemanualeandetheeworksheet.
Iteisehoped,ethisemanualemayebeeaeguidelineetoeimproveestudentelaboratoryeskilleespeciallyei
neinorganicelaboratoryework.




Yogyakarta,eAuguste2011




M.ePranjotoeUtomo




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, LaboratoryeManualeofePracticaleInorganiceIIeChemistry


RULESeOFeINORGANICeIIeLABORATORYeWORK


A. Laboratoryeworkepresence
1. Everyestudentemustecomeeonetimeeandefilletheepresenceebook.
2. Students,ewhoecomeeoverethane15eminutesefrometheelaboratoryeworkeschedule,emayefoll
owetheelaboratoryeworkeifeonlyepermittedebyetheelecturer.
3. Allestudentsemusteparticipateeineeveryelaboratoryeworkeactivity.
4. Theepermittedepracticaletagseareetwice.


B. CarryingeOuteofeLaboratoryeWork
1. LaboratoryeworkeofeInorganiceIIeisegroupelaboratoryeactivity.eEachegroupeconsistseof
4e students.e Eache groupe membere hase individuale responsibilitye toe thee resulte ofelaborator
yeworke(report).
2. Everyestudentehasetoewearewhite-laboratoryecoat,ebringeaenapkineandedropperepipette.


C. LaboratoryeWorkeReport
1. Everyestudentemustecomposeeindividualereporteonetheestudenteworksheet.
2. Studente worksheete muste bee collectede toe assistante ore lecturere ate thee samee daye withela
boratoryeworkeday.




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, LaboratoryeManualeofePracticaleInorganiceIIeChemistry


LABORATORYePRECAUTIONS
A. InsideetheeLaboratory
1. Doenoteeat,edrinkebeverageseorechewegumeinetheelaboratory.eDoenoteuseelaboratorye glas
swareeasecontainerseforefoodeorebeverages
2. Wearesafetyegoggleseandeaprons
3. Alwaysekeepetheeworkingeareaecleaneandeorderly
4. Knowetheelocationseandeoperatingeprocedureseofeallesafetyeequipment.
5. Notifyetheeinstructoreimmediatelyeofeanyeunsafeeconditioneyoueobserve
B. HandlingeChemicals
1. Allechemicalseinetheelaboratoryeareetoebeeconsiderededangerous.eDoenotetouch,etasteeores
melleanyechemicaleunlessespecificallyeinstructedetoedoeso
2. Checketheelabeleonechemicalebottlesetwiceebeforeeremovingeanyeofetheecontents.
3. Neverereturneunusedechemicalsetoetheireoriginalecontainers.
4. Acide muste bee handlede withe extremee care.e ALWAYSe ADDe ACIDe SLOWLYe TOe
WATER.
5. Handlee flammablee hazardouse liquidse overe ae pane toe containe spills.e Nevere dispenseefl
ammableeliquidseanywhereeneareaneopeneflameeoresourceeofeheat.
C. HandlingeglasswareeandeEquipment
1. Alwayse lubricatee glasswaree (tubing,e thistlee tubes,e thermometers,e etc.)e beforeeatt
emptingetoeinserteiteineaestopper.
2. Wheneremovingeaneelectricaleplugefromeitsesocket,egraspetheeplug,enotetheeelectricalecor
d.eKeepeyourehandsedryewheneworkingewitheelectricity.
3. Doenoteimmerseehoteglasswareeinecoldewater,eitemayeshatter.
4. Reportedamageeelectricaleequipmenteimmediately.
D. HeatingeSubstances
1. TURNeOFFeTHEeGASeATeGASeOUTLETeVALVEeaftereusing.
2. Nevereleaveeaeliteburnereunattended.eNevereleaveeanythingethateisebeingeheatedeoreisevis
iblyereactingeunattended.
3. Useetongseoreheat-protectiveeglovesewheneholdingeoretouchingeheatedeapparatus.




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