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Exam (elaborations)

ANALYTICAL CHEMISTRY EXERCISE

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Hi everyone, I hope you're doing well! I wanted to share some of the test papers I have for analytical chemistry practice, as I believe they could be helpful for revising important concepts and improving problem-solving skills. Feel free to go through them! All the best !

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FINAL TEST AS/JAN2023/CHM421




UNIVERSITI TEKNOLOGI MARA
_________________________________________________________________________
TIME : 2 HOURS
_________________________________________________________________________

QUESTION1

a) Define the purpose of standardization.
(1 mark)




b) Back titration is required in some chemical analysis as shown in chemical equation
below.

2HNO3 + CaCO3 Ca(NO3)2 + CO2 + H2O
HNO3 + NaOH NaNO3 + H2O

Sketch the titration curve for the above titration.
(2 marks)




c) A 15 mL water sample was titrated with 15.20 mL 0.003 M EDTA to the endpoint under
pH 10.

i) Discuss briefly why titration should not be performed at pH more than 10.

(2 marks)

, FINAL TEST AS/JAN2023/CHM421


ii) Calculate the hardness (ppm) of water by determining the content of MgCO3 in
a water sample.

(4 marks)




iii) Identify the level of hardness of the water sample based on value obtain in cii).
(1 mark)

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